| Research on Extraction Process of Eucommia Ulmoides Gum Based on Natural Deep Eutectic Solvents Pretreatment |
| Received:March 20, 2024 Revised:March 20, 2024 |
| DOI:10.12136/j.issn.1000-890X.2025.12.0946 |
| Key Words: Eucommia ulmoides gum;NADES;pretreatment;extraction process |
| Author Name | Affiliation | E-mail | | QU Pengkun* | Plant Conservation Technology Center,Guizhou Key Laboratory of Agricultural Biotechnology,Guizhou Academy of Agricultural Sciences | 1392149961@qq.com | | ZHAO Degang | Plant Conservation Technology Center,Guizhou Key Laboratory of Agricultural Biotechnology,Guizhou Academy of Agricultural Sciences | |
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| Abstract: |
| The extraction process conditions of Eucommia ulmoides gum using natural deep eutectic solvents(NADES) pretreatment were investigated.Based on single-factor test,orthogonal test and response surface test were employed to optimize the process.The results indicated that when NADES was composed by choline chloride/glucose with molar ratio of 1/2,the pretreatment temperature had the greatest effect on extraction rate of Eucommia ulmoides gum,followed by the material-to-liquid ratio and pretreatment time.The optimal pretreatment temperature obtained from the response surface test was 103 ℃,the material-to-liquid ratio was 1/22 g·mL-1,and the pretreatment time was 2.3 h,and the extraction rate of Eucommia ulmoides gum was 13.73% in verification test.On this basis,reflux extraction process was further optimized,and the best extraction time was 4 h,the extraction cycle was 1,and the solid-to-liquid ratio was 1/25 g·mL-1.Under the combined optimized conditions,the overall extraction rate of Eucommia ulmoides gum reached 14.85%.NADES pretreatment coupled with reflux extraction could significantly enhance the extraction efficiency of Eucommia ulmoides gum,providing reference for its efficient development and utilization. |
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